Intern
    Institut für Organische Chemie

    Bruker Avance III HD 600 (‘nmr600a‘)

    -   Single bay, installation 2014

    -   Oxford magnet, installation 1994

    -   SampleXpress automatic sample changer

    -   BCU 1 variable temperature precooling unit

    -   Cryo platform

    -   DCH 13C / 1H cryoprobe with z gradient and ATM

    -   Cryofit flow insert for HPLC hyphenation, 120 µl active volume

     

    -   Main applications:

    ·    1D and 2D NMR experiments with high sensitivity (cryoprobe), 0 to 80 °C

    ·    HPLC-NMR hyphenation

     

    Bruker Avance III HD 600 (‘nmr600b‘)

    -   Double bay, installation 2014

    -   Bruker Ascend magnet, installation 2014

    -   BACS 120 automatic sample changer

    -   BCU 2 variable temperature precooling unit for sample temperatures down to -55 °C

    -   Liquid nitrogen heat exchanger for lowest sample temperatures

    -   BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C

    -   10 mm 13C / 1H probe with z gradient and ATM, long term measurements up to 200 °C

    -   Equipment for diffusion measurements with pulsed field gradients up to 1800 G/cm:

        DIFF30L probe (1H inverse / 13C) and GREAT 60 A gradient amplifier

    -   3.2 mm MAS DVT probe, 15N to 31P / 1H + 19F

     

    -   Main applications:         

    ·    1D and 2D NMR experiments including heteronuclei

    ·    Variable temperature measurements

    ·    DOSY (i.a. large aggregates)

    ·    Solid state NMR (MAS)

     

    -   Spare probes for 600 MHz (purchase before 2005):

    ·    BBO probe with z gradient and ATM, 15N to 31P / 1H

    ·    TXI probe (1H inverse / 13C / 15N) with z gradient, without ATM

    ·    Dual probe (19F / 1H) without gradient, without ATM

    ·    10 mm BBO probe without gradient, without ATM, 109Ag to 31P / 1H

    ·    3 mm inverse (1H / 13C) HPLC NMR probe (60 µl active volume) with z gradient, without ATM

    ·    4 mm inverse (1H / 13C) HPLC NMR probe (120 µl active volume) without gradient, without ATM

     

    Bruker Avance III HD 400 (‘nmr400a‘)

    -   Nanobay, installation 2014

    -   Bruker Ultrashield magnet, installation 2000

    -   BACS 60 automatic sample changer

    -   BCU 05 variable temperature precooling unit

    -   BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C

     

    -   Main application:

    1D and 2D NMR experiments including heteronuclei

    (automation with ICON-NMR software)

     

    Bruker Avance III HD 400 (‘nmr400b‘)

    -   Nanobay, installation 2013

    -   Bruker Ascend magnet, installation 2013

    -   BACS 120 automatic sample changer

    -   BCU 2 variable temperature precooling unit for sample temperatures down to -60 °C

    -   Liquid nitrogen heat exchanger for lowest sample temperatures

    -   BBFO standard probe with z gradient and ATM, 15N to 31P + 19F / 1H, -150 to +150 °C

     

    -   Main applications:         

    ·    1D and 2D NMR experiments including heteronuclei

    (automation with ICON-NMR software)

    ·    Variable temperature measurements

     

    -   Spare probe for 400 MHz (purchase 2001):

             BBO with z gradient and ATM, 15N to 31P / 1H

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